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BIOASSAYS AND SCREENING METHODS



Drug discovery process:  Principles techniques and statergies used in new drug discovery.  High throughout screening. Human genomies robotics and economics of drug discovery, Regulations, for laboratory animal care and ethical requirements. 

 Bioassays : Basic principles of bioassays  official bioassays, experimental models and statistical designs employed in biological standardization. Biological  standardization of vaccines and sera with certain examples with reference to IP. Development of new bio assay methods.


 Preclinical  models employed in the screening of new drugs belonging to following categories.

Antifertility agents, sympathomimetics, parasympathomimetics, muscle relaxants (both central and peripheral). Sedatives, hypnotics, antiarrhythmic agents, cardiac stimulants, cardiotonic agents bronohodilators, antihistaminics, eicosanoids.

  Antipsychotic agents, antianxiety agents nootropic drugs antidepressant drugs; antiparkinsonism agents, anticpileptics; analgesics and anti-inflammatory agents; antiulcer agents; infarction; antiatherosclerotic drugs; antidiabetics; models for status epilepticus drugs. cerebroventricular and other newer techniques of drug administration and development; transgenic animals and other genetically prone animal models.


 Alternatives to animal screening procedures, cell-line handling and maintenance and propagation of cell lines, patch-clamp technique, in-vitro cell line based assays diabetics and arthraitis models, molecular biology techniques.


 Principles of toxicity evaluations, ED50, LD50 and TD values, International guidelines (ICH Ethics and animal experimentation recommendations).Guidelines and regulatory agencies – CPCSEA,OECD,FDA, FHSA,EPA,EEC,WHO etc,


 Introduction to biostatistics, parametric and non-parametric tests.  Regression and correlation: Linear regressions, Method of least squares; correlation coefficients, rank correlation, multiple regression Tests of significance: testing hypotheses, tests of significance based on normal distribution. t-test; significance of correlation coefficient. F-test and Analysis of Variance: 1-Way, 2-Way and 3-way classification, Chi-square test of (i) Variance of a normal population (ii) Goodness of fit, (iii) Independence in contingency tables. Non parametric tests, order statistics, sign test, run test, Median test.



BASIC PRINCIPLES OF TOXICOLOGY 
 

 General principal of regulatory toxicology. Use of animals in preclinical toxicology studies, role of preclinical toxicology in drug discovery and development process. Experimental considerations for assessing possible human risk. Flow chart for development of preclinical testing. Dose conversion factors, clinical signs toxicity.    
Single dose and repeat dose toxicity studies; Factors influencing such studies such as species, sex, size, route ,dose level; Data evaluation and regulatory requirements. Determination of Maximum Tolerated Dose (MTD) and LD 50 as per revised OECD guidelines. Allergenicity testing, dermal toxicity, immunotoxicology and in vitro methods of toxicology.  
         Reproductive toxicology assessment of male reproductive toxicity, spermatogenesis; Risk assessment in male reproductive toxicity; Female reproductive toxicology; Oocyte toxicity; alterations in reproductive endocrinology; Relationship between maternal and developmental toxicity.
Mutagenicity; Mechanisms of mutagenesis, point mutations,; Individual chromosomes and complete genome mutations, germ cell mutations, somatic cell mutation; Tests systems in vitro, chromosome damage and chromosomal aberration test, gene mutation, in vivo micronucleus tests in rodents, metaphase analysis.     
Preclinical toxicological requirements for biologicals and biotechnological products; safety analysis; problems specific to recombinant products, toxicokinetics, principles of GLP as per OECD guidelines for conducting preclinical toxicity studies

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